By K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler
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Additional resources for Analysis, Networks, Peptides
Analogous deformation stages can be observed during elongation at 343 K with the only difference that a somewhat better orientation of the polymer chains in the direction of stretch is observed at higher strains, Thus, the orientation function value of 0,85 at 280 ~ strain corresponds to an average inclination angle of the crystal c-axes with the draw direction of about 18 ° . Apart from orientational changes the evaluation of the polarization spectra in terms of the structural absorbance [see Eq.
34. Stress-strain diagrams of various crosslinked rubbers: (a) sulfur-crosslinked natural rubber (100 % 1,4-cis-polyisoprene)at 300 K, (b) sulfur-crosslinked natural rubber at 343 K, (c) radiationcrosslinked synthetic polyisoprene (93 % 1,4-cis-isomer)at 300 K (see text) 47 Rheo-Optical Fourier-Transform Infrared Spectroscopy The samples were prepared by microtoming from sheets of the polymers film sections which were 4 mm in width, 15 mm in length and about 100 ~tm in thickness. In the mechanical treatment the films were subjected to a loading-unloading cycle up to 530 % strain with an elongation and recovery rate of 85 ~ strain per minute and 12- to 15-scan spectra were taken in 9- to l 1-second intervals with a resolution of 4 cm-1.
Thus, it can be concluded that the shift of this band to 1475 cm -a in the spectrum of the drawn amorphous specimen is caused by a conformation in which the CH2-groups adjacent to the ester functionality deviate somewhat from the all-trans conformation of the almost planar, extended crystal form. Here too, a detailed picture of the response of amorphous PTMT film to the applied stress and any reversibility of the structural changes during uniaxial elongation and recovery in cyclic loading-unloading processes can be derived from simultaneous FTIR and mechanical measurements (Fig.
Analysis, Networks, Peptides by K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler