By K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler

ISBN-10: 0387136568

ISBN-13: 9780387136561

ISBN-10: 3540136568

ISBN-13: 9783540136569

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Additional resources for Analysis, Networks, Peptides

Example text

Analogous deformation stages can be observed during elongation at 343 K with the only difference that a somewhat better orientation of the polymer chains in the direction of stretch is observed at higher strains, Thus, the orientation function value of 0,85 at 280 ~ strain corresponds to an average inclination angle of the crystal c-axes with the draw direction of about 18 ° . Apart from orientational changes the evaluation of the polarization spectra in terms of the structural absorbance [see Eq.

34. Stress-strain diagrams of various crosslinked rubbers: (a) sulfur-crosslinked natural rubber (100 % 1,4-cis-polyisoprene)at 300 K, (b) sulfur-crosslinked natural rubber at 343 K, (c) radiationcrosslinked synthetic polyisoprene (93 % 1,4-cis-isomer)at 300 K (see text) 47 Rheo-Optical Fourier-Transform Infrared Spectroscopy The samples were prepared by microtoming from sheets of the polymers film sections which were 4 mm in width, 15 mm in length and about 100 ~tm in thickness. In the mechanical treatment the films were subjected to a loading-unloading cycle up to 530 % strain with an elongation and recovery rate of 85 ~ strain per minute and 12- to 15-scan spectra were taken in 9- to l 1-second intervals with a resolution of 4 cm-1.

Thus, it can be concluded that the shift of this band to 1475 cm -a in the spectrum of the drawn amorphous specimen is caused by a conformation in which the CH2-groups adjacent to the ester functionality deviate somewhat from the all-trans conformation of the almost planar, extended crystal form. Here too, a detailed picture of the response of amorphous PTMT film to the applied stress and any reversibility of the structural changes during uniaxial elongation and recovery in cyclic loading-unloading processes can be derived from simultaneous FTIR and mechanical measurements (Fig.

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Analysis, Networks, Peptides by K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler


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